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The [4+2] benzannulation reaction of internal or terminal alkynes with 2biaryl, 2heteroarylphenyl, or 2alkenylphenyl Grignard reagents in the presence of Fe(acac)(3), 4,4''ditertbutyl2,2''bipyridyl, and 1,2dichloro2methylpropane takes place at room temperature in 1 h to give 9substituted or 9,10disubstituted phenanthrenes and congeners
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obtained with a McCrone Micromill) (S1) with a Siemens D5000 Xray diffractometer. Powdered samples were scanned from 5 to 85 2 ! with steps of and a scanning time of 4 seconds.
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is a platform for academics to share research papers.
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The utilization of woodderived building blocks (xylochemicals) to replace fossilbased precursors is an attractive research subject of modern polymer science. Here, we demonstrate that bisguaiacol (BG), a ligninderived bisphenol analogue, can be used to prepare biobased polyesters with remarkable thermal
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